STT TÊN SẢN PHẨM CHỈ TIÊU TIÊU CHUẨN
PHÂN TÍCH THIẾT BỊ
PHÂN TÍCH HÓA CHẤT CHUẨN Thông số Cột Sắc Ký Đầu dò GC Khí mang GC KHÁC (Vật dụng)
1 Magnesium stearate Thành phần
acid béo DĐVN IV GC 1/ Dung dịch boron
trifluoride-methanol
2/ Heptan
3/ Natri clorid
4/ Natri sulfat khan 1/ Palmitic acid
2/ Stearic acid Silica (30m x 0,32 mm)
được tráng với macrogol 20000 (độ dày lớp phim 0,5 um) FID Helium
2 Polysorbat 60 Thành phần
acid béo BP 2014 GC Methanolic Sodium Hydroxide, boron trifluoride , heptane, sodium chloride , sodium sulfate, Nu-Chek mixture 19A,
Nu-Chek mixture 17A,
stearic acid, palmitic
acid, and oleic acid Fused silica
(30m x 0,32mm); macrogol 20000; 0,5um FID Helium
Ethylene và
dioxan BP 2014 GC polyethylene glycol 200 R1, Acetaldehyde, dimethylacetamide 1/ Ethylen oxide
2/ Dioxan
3/ Acetaldehyde Fused silica
(50m x 0,53mm); poly(dimethyl)(diphenyl)siloxane R (5 µm) FID Helium Headspace,
Sau khi nâng tiêu chuẩn lên BP 2017 sẽ có chỉ tiêu này.
3 Ethanol 96% Tạp chất
bay hơi DĐVN IV GC 4-methylpentan-2-ol
acetal (1,1-diethoxyethan)
Methanol
Benzen 1/ Methanol khan
2/ Acetaldehyd
3/ Benzen Silica nung chảy, (30 m ´ 0,32 mm)
được nhồi poly[(cyanopropyl)
(phenyl)] [dimethyl]siloxan
(độ dày lớp bao 1,8 mm) FID Helium
4 Soyabean oil Thành phần
acid béo USP38 GC Methanolic Sodium Hydroxide, boron trifluoride , heptane, sodium chloride , sodium sulfate, Nu-Chek mixture 19A, Nu-Chek mixture 17A, stearic acid, palmitic acid, and oleic acid a 0.53-mm × 30-m fused-silica capillary column bonded with a 1.0-µm layer of phase G16 FID Helium
Sterol USP38 GC + LC chlorotrimethylsilane,
bis(trimethylsilyl)trifluoroacetamide,
sunflower oil, cholesterol, ether,
potassium hydroxide, ethanol 0.25-mm × 30-m fused-silica capillary; 0.25-µm layer of phase G27 Helium
5 Hydrogenated castor oil Thành phần
acid béo USP 39 GC 1,1-dimethylethyl methyl ether R1 methyl stearate CRS, methyl 12-hydroxystearate CRS l = 30 m; Ø = 0.25 mm; macrogol 20 000 R (film thickness 0.25 µm). FID Helium
6 CETOSTEARYL ALCOL Định lượng DĐVN IV GC ethanol cetyl alcol , stearyl alcol Cột thép không gỉ (3 m × 4 mm) được nhồi diatomit dùng cho sắc ký khí (TT) đã tẩm 10 % (kl/kl) poly-(dimethyl)siloxan (TT) FID Nitrogen
7 Macrogol Cetostearyl Ether A6 Ethylene Oxide and Dioxan BP2013 GC polyethylene glycol 200 R1, Acetaldehyde, dimethylacetamide dioxan stock solution, ethylene oxide stock solution , a capillary glass or quartz column 30 m long and 0.32 mm in internal diameter the inner surface of which is coated with a 1.0 µm thick layer of poly(dimethyl)siloxane R, FID Helium/Nitrogen Headspace
8 Macrogol Cetostearyl Ether A25 Ethylene Oxide and Dioxan BP2013 GC polyethylene glycol 200 R1, Acetaldehyde, dimethylacetamide dioxan stock solution, ethylene oxide stock solution , a capillary glass or quartz column 30 m long and 0.32 mm in internal diameter the inner surface of which is coated with a 1.0 µm thick layer of poly(dimethyl)siloxane R, FID Helium/Nitrogen Headspace
9 CETYL ALCOL Định tính + Định lượng BP2014 GC ethanol, stearyl alcohol cetyl alcol l = 30 m, Ø = 0.32 mm, stationary phase: poly(dimethyl)siloxane R (1 µm) FID Helium
10 Stearyl alcohol Định tính + Định lượng BP2014 GC ethanol, cetyl alcohol stearyl alcol l = 30 m, Ø = 0.32 mm, stationary phase: poly(dimethyl)siloxane R (1 µm) FID Helium
11 Glycerin Tạp A và tạp liên quan BP 2013 GC diethylene glycol Glycerol l = 30 m, Ø = 0.53 mm; stationary phase: 6 per cent polycyanopropylphenyl siloxane and 94 per cent of polydimethylsiloxane. FID Helium
12 Levocetirizine Dung môi tồn dư TC NSX GC Acetone, DMF, Toluene, Methanol, MDC USP Class 1 Residual Solvents Mixture RS, USP Residual Solvents Class 2 a 0.32-mm × 30-m fused-silica column coated with a 1.8-µm layer of phase G43 or a 0.53-mm × 30-m wide-bore column coated with a 3.0-µm layer of phase G43 FID Helium/Nitrogen Headspace
13 Milk thistle extract Dung môi tồn dư USP 38 GC Acetone USP Class 1 Residual Solvents Mixture RS, USP Residual Solvents Class 3 a 0.32-mm × 30-m fused-silica column coated with a 1.8-µm layer of phase G43 or a 0.53-mm × 30-m wide-bore column coated with a 3.0-µm layer of phase G43 FID Helium/ Nitrogen Headspace
Thuốc trừ sâu GC + LC acetone, carbophenothion Aldrin and dieldrin, DDT, Endrin 0.32-mm × 30-m fused silica column coated with a 0.25-µm layer of phase G1 ECD Hydrogen/
Helium/
Nitrogen
14 Ivermectin Ethanol + formamide DĐVN IV GC Propanol, m-xylen, ethanol ethanol, formamide fused silica; size: l = 30 m, Ø = 0.53 mm; stationary phase: macrogol 20 000 R (film thickness 1 µm) FID Helium
15 Omega 3 fish oil EPA + DHA USP GC butylated hydroxytoluene , isooctan, methyl palmitate, methyl stearate, methyl arachidate, methyl behenate,ocosahexaenoic acid methyl ester , tetracos-15-enoic acid (nervonic acid) methyl ester USP Fish oilil RS, USP Methyl Tricosanoate RS, USP Docosahexaenoic Acid Ethyl Esters RS, USP Eicosapentaenoic Acid Ethyl Esters RS, 0.25-mm × 25-m fused–silica capillary column bonded with a 0.20-µm film of phase G16 FID Helium
16 Menthol Tạp liên quan DĐVN IV GC methylen clorid Menthol, isomenthol, Cột thủy tinh (2,0 m × 2 mm) được nhồi diatomit dùng cho sắc ký khí và được tẩm 15 % (kl/kl) macrogol 1500 FID Nitrogen
17 Carbomer 940 Benzen USP34 GC sodium chloride, methanol benzen 0.53-mm × 30-m fused silica, coated with 3.0-µm G43 FID Helium
18 Gentamycin sulfate Methanol USP 38 GC dimethyl sulfoxid , methanol, Cột mao quản thủy tinh hoặc
cột có nòng rỗng, dài 30 m
có đường kính trong 0,32 mm
hoặc 0,53 mm, được phủ
macrogol 20 000 dày 0,25 mm. FID/
MS Helium/Nitrogen Headspace
19 Sorbitan monostearate Thành phần
acid béo BP 2013 GC heptane, sodium chloride , sodium sulfate, potassium hydroxide mixture of calibrating substances with the composition ester fused silica; l = 30 m,
Ø = 0.32 mm; stationary phase:
macrogol 20 000 R
(film thickness 0.5 µm) FID Helium
20 Low-Substituted
Hydroxypropyl Cellulose Định lượng USP 38 GC Hydriodic acid, adipic acid, o-xylene, isopropyl iodide n-octane, 3–4-mm × 1.8–3-m glass, packed
with 20% liquid phase G28 on
100–120 mesh support S1C
that is not silanized. HydrogenFID/
TCD Helium Bên ngoài
không nhận
21 Lacidipine propan-2-ol BP2013 GC dioxan, dimethylformamide propan-2-ol thủy tinh polymethylsiloxan hoặc CP-Sil 5CB (60 m x 0,32 mm; 5 µm) FID Helium
22 Triethanolamine Tạp liên quan BP2013 GC 3-aminopropanol R , trolamine poly(dimethyl)(diphenyl)siloxane R FID Helium
Tạp C acetone R, chloroform, kieselguhr for chromatography , potassium carbonate R, N-nitrosodiisopropanolamine, methanol base-deactivated poly(dimethyl)(diphenyl)siloxane R CL Helium
23 Diethylene Glycol Monoethyl Ether Định lượng USP 38 GC 2-methoxyethanol, 2-ethoxyethanol, ethylene glycol, diethylene glycol, and USP Diethylene Glycol Monoethyl Ether RS 0.32-mm × 30-m fused-silica bonded with a 1.0-µm layer of phase G46 FID Helium
Ethylene Oxide ethylene oxide, acetaldehyde 0.32-mm × 30-m glass or quartz capillary bonded with a 1.0-µm layer of phase G1 FID Helium Headspace
24 Glucosamine Tạp chất bay hơi USP 30 GC l = 30 m; Ø = 0.25 mm; macrogol 20 000 R (film thickness 0.25 µm). FID Helium Headspace
25 Xylitol Tạp + ĐL EP 8.0 GC poly(cyanopropylphenyl)(14)(methyl)(86)siloxane R (0.25 µm) FID Nitrogen
26 Dl tocopheryl acetate tạp + DL BP 2013 GC poly(dimethyl)siloxane R (film thickness 0.25 µm) FID Nitrogen